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- February 27, 2011, 02:55:21 PMShujin process improvement solution
_ ÷ sterilization. ÷ _ ÷ deployment heat reflux extraction finished _ ÷ wash cutting raw herbs, dried - ÷ net material heat reflux extraction - ÷ _ ÷ filtered liquor filtrate recycle filtrate standing _ ÷ _} _ ÷ deployment of finished diatomite 2 cycles solvent selection process selection 2.2.1 2.2 prescriptions in the composition of the active ingredients such as Millettia alkaloid glycosides,You are not allowed to view links. Register or Login, solvent ethanol concentration 5O ~ 70 when it has a strong leaching of choice. Ma currently the magic and so contains a lot of free anthracene quinone,You are not allowed to view links. Register or Login, anthraquinone glycosides. Concentration of ethanol below 50 when a 2.11.01.1I. 5 photos Extraction Time and extract the 2.2.3 coordinate rash Ha extraction temperature selected in the above experiment, we found the extraction temperature higher than 90 moderate. 2.2.4 Conditions for filter filters take into account the influence of factors, take filter temperature,You are not allowed to view links. Register or Login, filter cycle time, the amount of diatomaceous earth as a study of factors,You are not allowed to view links. Register or Login, the level design table for cable, see Table 2. Results show that the extraction temperature A3B3Cg z5 ℃ ~ 35 Table 3. Table 2, the level of form factors bar officials experimental table 3 are the results of 2.3 in summer the total solid product quality standards 2.3.1 Comparison of the two processes were taken 3 batches of finished liquid 50ml by version of Appendix A wine agent detection under the first method of total solids,You are not allowed to view links. Register or Login, and the results showed that the infiltration heat reflux extraction residue than the finished production of the total solid content increased by 46.4, Table 4. Table 4 Comparison product total rounded heat back to the sneeze camp irrigation method to extract total solids (g) o.351n4135o.5o51o.5902o.6146o.6461 Jian is a solid o.70. .83. Ol.18m.29I) 471.242.3.2 total extract Comparing the two extraction stability of the production total of 12 batches of extract to do the number of statistics. infiltration of a 17.02x x = 28.43S permeability = 20.97S back Back = 0.666 ie CV = s infiltration infiltration / X infiltration × 100 = 20.97/I7.02 × 100 = 123.26CV back = S Back / X back to the × 100 = 0.666/28.43 × 100 = 2.30CV infiltration method ≥ 5 shows percolation process instability. CV back <15oA that reflux process is relatively stable. 2.3.3 Comparison of sediment was taken two processes 3 batches of finished product each 500ml liquid precipitation observer in the home at 2 ℃ ~ 7 ℃ standing next 100 days, the results shown in Table 5. Table 5 sediment was observed Table Note: Percentage of precipitation: (precipitation amount ÷ 5oo) xioo data show that the production of heat reflux extraction liquid precipitation is less than the finished production of the finished product percolation volume of liquid precipitation, while the total extract was significantly higher infiltration method in the bowl. 2.3.4 Comparison of the main active ingredient by Lidermahh, Kedde, magnesium acetate reaction and determination of total alkaloids showed that the heat reflux extraction liquid finished products contained saponins, cardiac glycosides, anthraquinones and total alkaloid content infiltration than the production of the finished bowl of the liquid component content is higher. 2.4 The process cycle, labor productivity compared to the infiltration slag from drying to the deployment of sterilization process is completed before totaling 164h, and reflux from the deployment of cutting to the front after just 21.5h, with deployment of filter 2 .5 h, totaling 84h, shorten the process cycle of 140h. Reflux extraction line 18 a month can produce 22 million bottles of the product, while the infiltration bowl method a total of 30 production lines, monthly production of 80,000 bottles of the product. Back to the lake for a labor rate production of 22 million bottles / 18 million bottles a l_22 / production of human labor percolation rate = 80000 bottles / 30 of a 02,600 bottle | labor productivity ratio = 1.22 / 0. 3 Summary of 26 = 4.58 times the experiments show that heat reflux extraction method Shujin solution available to improve the quality of their products, while improving labor efficiency, diatomaceous earth filtration cycle was less than the finished product not only precipitation infiltration bowl Law precipitation amount, but also eliminates sterilization process, practice proved that the process finished after the average number of bacteria solution of 50 / 100ml, meet the At the same time production of liquor agents is due back in the closed pipe production, is conducive to improving the quality of products and companies within the GMP standards.
_ ÷ sterilization. ÷ _ ÷ deployment heat reflux extraction finished _ ÷ wash cutting raw herbs, dried - ÷ net material heat reflux extraction - ÷ _ ÷ filtered liquor filtrate recycle filtrate standing _ ÷ _} _ ÷ deployment of finished diatomite 2 cycles solvent selection process selection 2.2.1 2.2 prescriptions in the composition of the active ingredients such as Millettia alkaloid glycosides,You are not allowed to view links. Register or Login, solvent ethanol concentration 5O ~ 70 when it has a strong leaching of choice. Ma currently the magic and so contains a lot of free anthracene quinone,You are not allowed to view links. Register or Login, anthraquinone glycosides. Concentration of ethanol below 50 when a 2.11.01.1I. 5 photos Extraction Time and extract the 2.2.3 coordinate rash Ha extraction temperature selected in the above experiment, we found the extraction temperature higher than 90 moderate. 2.2.4 Conditions for filter filters take into account the influence of factors, take filter temperature,You are not allowed to view links. Register or Login, filter cycle time, the amount of diatomaceous earth as a study of factors,You are not allowed to view links. Register or Login, the level design table for cable, see Table 2. Results show that the extraction temperature A3B3Cg z5 ℃ ~ 35 Table 3. Table 2, the level of form factors bar officials experimental table 3 are the results of 2.3 in summer the total solid product quality standards 2.3.1 Comparison of the two processes were taken 3 batches of finished liquid 50ml by version of Appendix A wine agent detection under the first method of total solids,You are not allowed to view links. Register or Login, and the results showed that the infiltration heat reflux extraction residue than the finished production of the total solid content increased by 46.4, Table 4. Table 4 Comparison product total rounded heat back to the sneeze camp irrigation method to extract total solids (g) o.351n4135o.5o51o.5902o.6146o.6461 Jian is a solid o.70. .83. Ol.18m.29I) 471.242.3.2 total extract Comparing the two extraction stability of the production total of 12 batches of extract to do the number of statistics. infiltration of a 17.02x x = 28.43S permeability = 20.97S back Back = 0.666 ie CV = s infiltration infiltration / X infiltration × 100 = 20.97/I7.02 × 100 = 123.26CV back = S Back / X back to the × 100 = 0.666/28.43 × 100 = 2.30CV infiltration method ≥ 5 shows percolation process instability. CV back <15oA that reflux process is relatively stable. 2.3.3 Comparison of sediment was taken two processes 3 batches of finished product each 500ml liquid precipitation observer in the home at 2 ℃ ~ 7 ℃ standing next 100 days, the results shown in Table 5. Table 5 sediment was observed Table Note: Percentage of precipitation: (precipitation amount ÷ 5oo) xioo data show that the production of heat reflux extraction liquid precipitation is less than the finished production of the finished product percolation volume of liquid precipitation, while the total extract was significantly higher infiltration method in the bowl. 2.3.4 Comparison of the main active ingredient by Lidermahh, Kedde, magnesium acetate reaction and determination of total alkaloids showed that the heat reflux extraction liquid finished products contained saponins, cardiac glycosides, anthraquinones and total alkaloid content infiltration than the production of the finished bowl of the liquid component content is higher. 2.4 The process cycle, labor productivity compared to the infiltration slag from drying to the deployment of sterilization process is completed before totaling 164h, and reflux from the deployment of cutting to the front after just 21.5h, with deployment of filter 2 .5 h, totaling 84h, shorten the process cycle of 140h. Reflux extraction line 18 a month can produce 22 million bottles of the product, while the infiltration bowl method a total of 30 production lines, monthly production of 80,000 bottles of the product. Back to the lake for a labor rate production of 22 million bottles / 18 million bottles a l_22 / production of human labor percolation rate = 80000 bottles / 30 of a 02,600 bottle | labor productivity ratio = 1.22 / 0. 3 Summary of 26 = 4.58 times the experiments show that heat reflux extraction method Shujin solution available to improve the quality of their products, while improving labor efficiency, diatomaceous earth filtration cycle was less than the finished product not only precipitation infiltration bowl Law precipitation amount, but also eliminates sterilization process, practice proved that the process finished after the average number of bacteria solution of 50 / 100ml, meet the At the same time production of liquor agents is due back in the closed pipe production, is conducive to improving the quality of products and companies within the GMP standards.